XAFS Techniques for Catalysts, Nanomaterials, and Surfaces

XAFS Techniques for Catalysts, Nanomaterials, and Surfaces PDF

Author: Yasuhiro Iwasawa

Publisher: Springer

Published: 2016-10-19

Total Pages: 545

ISBN-13: 3319438662

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This book is a comprehensive, theoretical, practical, and thorough guide to XAFS spectroscopy. The book addresses XAFS fundamentals such as experiments, theory and data analysis, advanced XAFS methods such as operando XAFS, time-resolved XAFS, spatially resolved XAFS, total-reflection XAFS, high energy resolution XAFS, and practical applications to a variety of catalysts, nanomaterials and surfaces. This book is accessible to a broad audience in academia and industry, and will be a useful guide for researchers entering the subject and graduate students in a wide variety of disciplines.

X-ray Absorption Fine Structure for Catalysts and Surfaces

X-ray Absorption Fine Structure for Catalysts and Surfaces PDF

Author: Yasuhiro Iwasawa

Publisher: World Scientific

Published: 1996

Total Pages: 438

ISBN-13: 9789810223236

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X-ray absorption fine structure (XAFS) is a powerful technique in characterization of structures and electronic states of materials in many research fields including, e.g., catalysts, semiconductors, optical ingredients, magnetic materials, and surfaces. This characterization technique could be applied in a static or a dynamic state (in-situ condition). The XAFS can provide information that is not accessible by other techniques for characterization of materials, particularly catalysts and related surfaces. Furthermore, XAFS can provide a molecular-level approach to the study of reaction mechanisms for the understanding of catalysts and development of new catalysts. A number of synchrotron radiation facilities have been planned to be built in Asian countries in addition to the high-brilliant synchrotron radiation facilities under construction in the USA, Europe, and Japan. The applications of XAFS have now expanded to catalytic chemistry and engineering, surface science, organometallic chemistry, materials science, solid-state chemistry, geophysics, etc. This book caters to a wide range of researchers and students working in the domain or related topics.

International Tables for Crystallography, Volume I

International Tables for Crystallography, Volume I PDF

Author: Christopher Chantler

Publisher: John Wiley & Sons

Published: 2024-08-19

Total Pages: 1090

ISBN-13: 1119433940

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X-ray absorption spectroscopy and X-ray emission spectroscopy are complementary to crystallographic methods, particularly for materials science and the study of nanostructure and systems with partial disorder and partial local order, including solutions, gases, liquids, glasses and powders. This new volume of International Tables for Crystallography has nine parts and over 150 chapters contributed by a wide range of international experts. Part 1 provides a brief overview and introduction to the background of X-ray absorption spectroscopy (XAS) and experimental facilities. Part 2 discusses the quantum theory of XAS and related approaches. Part 3 describes both standard and advanced experimental methods used in XAS, X-ray emission spectroscopy (XES) and related techniques. Part 4 covers both standard and more advanced pre-processing of data. Part 5 gives an extensive overview of the analysis of experimental data. Part 6 provides details of the major software packages for data collection, reduction and analysis. Part 7 outlines the importance in science, reporting and hypothesis testing of the exchange of input and processed output data, and data deposition. It also presents excerpts of tables of data and supplementary material for XAS, pre-edge studies, X-ray absorption near-edge spectroscopy (XANES) and X-ray absorption fine structure (XAFS) studies. These tables are also available in full as online supporting information. Part 8 explores a wide range of applications of XAS in fields including materials science, physics, chemistry, biology, earth sciences, catalysis and cultural heritage. Part 9 presents definitions of the terms and quantities used, as developed by the International Union of Crystallography's Commission on XAFS. The volume has been written for the worldwide XAS community of thousands of practitioners, beamline scientists, experts and academics, and for the novice user who wishes to know what XAS and XES can do for them and how they may use these techniques for their particular purposes. The volume is therefore intended to be a self-contained, authoritative reference work that can also be used for training, learning or teaching, providing practical guidance for readers of all levels of experience. More information on the volumes in the series International Tables for Crystallography can be found at https://it.iucr.org.

Advanced Characterization Of Nanostructured Materials: Probing The Structure And Dynamics With Synchrotron X-rays And Neutrons

Advanced Characterization Of Nanostructured Materials: Probing The Structure And Dynamics With Synchrotron X-rays And Neutrons PDF

Author: Sunil K Sinha

Publisher: World Scientific

Published: 2021-03-23

Total Pages: 430

ISBN-13: 9811231524

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Advanced Characterization of Nanostructured Materials — Probing the Structure and Dynamics with Synchrotron X-Rays and Neutrons is a collection of chapters which review the characterization of the structure and internal dynamics of a wide variety of nanostructured materials using various synchrotron X-ray and neutron scattering techniques. It is intended for graduate students and researchers who might be interested in learning about and applying these methods. The authors are well-known practitioners in their fields of research who provide detailed and authoritative accounts of how these techniques have been applied to study systems ranging from thin films and monolayers on solid surfaces and at liquid-air, liquid-liquid and solid-liquid interfaces; nanostructured composite materials; battery materials, and catalytic materials. While there have been a great many books published on nanoscience, there are relatively few that have discussed in one volume detailed synchrotron X-ray and neutron methods for advanced characterization of nanomaterials in thin films, composite materials, catalytic and battery materials and at interfaces. This book should provide an incentive and a reference for researchers in nanomaterials for using these techniques as a powerful way to characterize their samples. It should also help to popularize the use of synchrotron and neutron facilities by the nanoscience community.

Compendium of Surface and Interface Analysis

Compendium of Surface and Interface Analysis PDF

Author: The Surface Science Society of Japan

Publisher: Springer

Published: 2018-02-19

Total Pages: 807

ISBN-13: 9811061564

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This book concisely illustrates the techniques of major surface analysis and their applications to a few key examples. Surfaces play crucial roles in various interfacial processes, and their electronic/geometric structures rule the physical/chemical properties. In the last several decades, various techniques for surface analysis have been developed in conjunction with advances in optics, electronics, and quantum beams. This book provides a useful resource for a wide range of scientists and engineers from students to professionals in understanding the main points of each technique, such as principles, capabilities and requirements, at a glance. It is a contemporary encyclopedia for selecting the appropriate method depending on the reader's purpose.

Nanosensors for Smart Cities

Nanosensors for Smart Cities PDF

Author: Baoguo Han

Publisher: Elsevier

Published: 2020-02-13

Total Pages: 962

ISBN-13: 0128199237

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Nanosensors for Smart Cities covers the fundamental design concepts and emerging applications of nanosensors for the creation of smart city infrastructures. Examples of major applications include logistics management, where nanosensors could be used in active transport tracking devices for smart tracking and tracing, and in agri-food productions, where nanosensors are used in nanochips for identity, and food inspection, and smart storage. This book is essential reading for researchers working in the field of advanced sensors technology, smart city technology and nanotechnology, and stakeholders involved in city management. Nanomaterials based sensors (nanosensors) can offer many advantages over their microcounterparts, including lower power consumption, high sensitivity, lower concentration of analytes, and smaller interaction distance between object and sensor. With the support of artificial intelligence (AI) tools, such as fuzzy logic, genetic algorithms, neural networks, and ambient-intelligence, sensor systems are becoming smarter. Provides information on the fabrication and fundamental design concepts of nanosensors for intelligent systems Explores how nanosensors are being used to better monitor and maintain infrastructure services, including street lighting, traffic management and pollution control Assesses the challenges for creating nanomaterials-enhanced sensors for mass-market consumer products

Amorphous Nanomaterials

Amorphous Nanomaterials PDF

Author: Lin Guo

Publisher: John Wiley & Sons

Published: 2021-03-30

Total Pages: 432

ISBN-13: 3527826343

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A valuable overview covering important fundamental and applicative aspects of amorphous nanomaterials! Amorphous nanomaterials are very important in non-crystalline solids, which have emerged as a new category of advanced materials. Compared to the crystalline counterpart, amorphous nanomaterials with isotropic nature always exhibit fast ion diffusion, relieved strain, and higher reactivity, enabling such materials to exhibit high performance in mechanics and catalysis, as well as other interesting properties. Amorphous Nanomaterials: Preparation, Characterization, and Applications covers the fundamental concept, synthesis, characterization, properties, and applications of nanoscaled amorphous materials. It starts with the introduction of amorphous materials, then gives a global view of the history, structure, and growth mechanism of amorphous nanomaterials. Subsequently, some powerful techniques to characterize amorphous materials, such as X-ray absorption fine structure spectroscopy, spherical aberration electron microscope, in-situ-Transmission Electron Microscope, Electron Energy Loss Spectroscopy, and some other defect characterization technologies are included. Furthermore, the emerging innovative methods to fabricate well-defined, regularshaped amorphous nanomaterials, including zero-, one-, two-, and three-dimensional amorphous nanomaterials are systematically introduced. The fascinating properties and applications related to amorphous nanomaterials including the applications in electrocatalysis, batteries, supercapacitors, photocatalysis, mechanics, etc., are presented. It will greatly help the researchers to find professional answers related to amorphous materials. Great topic: amorphous nanomaterials are a very large and important field in both academia and industry Comprehensive: in-depth discussion of various important aspects, from both a fundamental and an applied point of view, on the chemistry, physics and technological importance of the amorphous nanomaterials are presented Vitally needed: the understanding of the fundamentals of amorphous nanomaterials is a prerequisite for devising new applications of such materials Highly relevant: amorphous nanomaterials have found specific applications in chemistry, catalysis, physics, sensing, batteries, supercapacitors, and engineering Amorphous Nanomaterials is a vital resource for materials scientists, inorganic and physical chemists, solid state chemists, physicists, catalytic and analytical chemists, as well as organic chemists.

X-ray and Neutron Techniques for Nanomaterials Characterization

X-ray and Neutron Techniques for Nanomaterials Characterization PDF

Author: Challa S.S.R. Kumar

Publisher: Springer

Published: 2016-10-13

Total Pages: 830

ISBN-13: 3662486067

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Fifth volume of a 40 volume series on nanoscience and nanotechnology, edited by the renowned scientist Challa S.S.R. Kumar. This handbook gives a comprehensive overview about X-ray and Neutron Techniques for Nanomaterials Characterization. Modern applications and state-of-the-art techniques are covered and make this volume an essential reading for research scientists in academia and industry.

Modern Developments In Catalysis, Volume 2

Modern Developments In Catalysis, Volume 2 PDF

Author: Graham J Hutchings

Publisher: World Scientific

Published: 2023-02-06

Total Pages: 640

ISBN-13: 1800612028

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The UK Catalysis Hub is a consortium of universities working together on fundamental and applied research to find out how catalysts work and to improve their effectiveness. The contribution of catalysis to manufacturing contributes to almost 40% of global GDP, making development and innovation within the field integral to industry.Modern Developments in Catalysis, Volume 2 provides a review and update of current research and practice on catalysis. Topics range from the treatment of water using novel techniques for carbon neutrality, cutting-edge techniques using intense radiation including Operando Synchrotron Infrared Microspectroscopy to innovation in homogeneous catalysis, heterogeneous catalysis and biocatalysis. Edited by leaders of the UK Hub, this book provides insight into one of the most important areas of modern chemistry — it represents a unique learning opportunity for students and professionals studying and working towards speeding up, improving and increasing the rate of catalytic reactions in science and industry.

Nanotechnology in Catalysis

Nanotechnology in Catalysis PDF

Author: Bert Sels

Publisher: John Wiley & Sons

Published: 2017-06-21

Total Pages: 1500

ISBN-13: 3527699813

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Reflecting the R&D efforts in the field that have resulted in a plethora of novel applications over the past decade, this handbook gives a comprehensive overview of the tangible benefits of nanotechnology in catalysis. By bridging fundamental research and industrial development, it provides a unique perspective on this scientifically and economically important field. While the first three parts are devoted to preparation and characterization of nanocatalysts, the final three provide in-depth insights into their applications in the fine chemicals industry, the energy industry, and for environmental protection, with expert authors reporting on real-life applications that are on the brink of commercialization. Timely reading for catalytic chemists, materials scientists, chemists in industry, and process engineers.