Structural Studies of Polymers by Solution Nmr

Structural Studies of Polymers by Solution Nmr PDF

Author: H.N. Cheng

Publisher: iSmithers Rapra Publishing

Published: 2001

Total Pages: 168

ISBN-13: 9781859572481

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Solution-state NMR spectroscopy is generally regarded as the premier technique to characterise polymer structure. This report provides a timely review of the developments in the NMR of polymers in solution in the past few years. An additional indexed section containing several hundred abstracts from the Polymer Library gives useful references for further reading.

NMR of Polymers

NMR of Polymers PDF

Author: Frank A. Bovey

Publisher: Academic Press

Published: 1996-11-19

Total Pages: 471

ISBN-13: 0080537588

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NMR has made important contributions to our understanding of structure–property relationships in polymers. This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new solution and solid-state methods in polymer science. NMR of Polymers is written by leading authorities for graduate students and professionals in academia and industry. Provides comprehensive overview of NMR in Polymer Science Covers multidimensional NMR Includes new solution and solid state methods Addresses chain conformation and dynamics

Solid State NMR of Polymers

Solid State NMR of Polymers PDF

Author: T. Asakura

Publisher: Elsevier

Published: 1998-08-03

Total Pages: 1017

ISBN-13: 0080541461

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In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods. This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described. Features of this book: • Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field • Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists. This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.

NMR Spectroscopy of Polymers

NMR Spectroscopy of Polymers PDF

Author: Tatsuki Kitayama

Publisher: Springer Science & Business Media

Published: 2013-03-09

Total Pages: 231

ISBN-13: 3662089823

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Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.

Nuclear Magnetic Resonance

Nuclear Magnetic Resonance PDF

Author: G A Webb

Publisher: Royal Society of Chemistry

Published: 2007-10-31

Total Pages: 588

ISBN-13: 1847553885

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As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Solid State NMR Spectroscopy for Biopolymers

Solid State NMR Spectroscopy for Biopolymers PDF

Author: Hazime Saitô

Publisher: Springer Science & Business Media

Published: 2006-08-05

Total Pages: 455

ISBN-13: 1402043031

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‘‘Biopolymers’’ are polymeric materials of biological origin, including globular, membrane, and fibrous proteins, polypeptides, nucleic acids, po- saccharides, lipids, etc. and their assembly, although preference to respe- ive subjects may be different among readers who are more interested in their biological significance or industrial and/or medical applications. Nevert- less, characterizing or revealing their secondary structure and dynamics may be an equally very important and useful issue for both kinds of readers. Special interest in revealing the 3D structure of globular proteins, nucleic acids, and peptides was aroused in relation to the currently active Structural Biology. X-ray crystallography and multidimensional solution NMR sp- troscopy have proved to be the standard and indispensable means for this purpose. There remain, however, several limitations to this end, if one intends to expand its scope further. This is because these approaches are not always straightforward to characterize fibrous or membrane proteins owing to extreme difficulty in crystallization in the former, and insufficient spectral resolution due to sparing solubility or increased effective molecular mass in the presence of surrounding lipid bilayers in the latter.

The NMR of Polymers

The NMR of Polymers PDF

Author: I. Ya Slonim

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 366

ISBN-13: 1468417738

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In the time since this book was written, the application of NMR in the study of polymers has continued to develop rapidly. The main trends of the work have remained as before, namely, the study of the structure of polymers, molecular motion in them, and chemical conversions of high-molecular-weight substances. How ever, as a result of the refinement of experimental techniques and development of the theory, new progress has been achieved, par ticularly in the NMR spectroscopy of polymer solutions. We therefore decided that it was worthwhile to provide an ad ditionallist of literature, covering papers published in 1965, 1966, and the beginning of 1967. By using the bibliographic directory appended to the list, the reader can readily find references to the latest literature for all sections of the book. I. Ya. Slonim A. N. Lyubimov v Preface to the Russian Edition The aim of this book is mainly to answer the questions which inevitably arise for a chemist who wishes to use NMR in his work on polymers.

Analysis of Thermoset Materials, Precursors and Products

Analysis of Thermoset Materials, Precursors and Products PDF

Author: Martin J. Forrest

Publisher: iSmithers Rapra Publishing

Published: 2003

Total Pages: 164

ISBN-13: 9781859573907

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This report presents an overview of the chemical analysis of thermosets. Materials based on thermosets present the analyst with considerable challenges due to their complexity and the wide range of polymer types and additives available. This review sets out to present an introduction to the analytical techniques and methods that are used to characterise and carry out quality control work on thermosets, investigate the failure of thermosets products and to deformulate thermoset compounds. The review is accompanied by around 400 abstracts from papers and books in the Rapra Polymer Library database, to facilitate further reading on this subject.

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