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Spectrometric Identification of Organic Compounds

Author: Robert Milton Silverstein

Publisher:

Published: 2005

Total Pages: 0

ISBN-13: 9780471429135

Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist

Spectrometric Identification of Organic Compounds

Author: Robert M. Silverstein

Publisher: John Wiley & Sons

Published: 2014-09-29

Total Pages: 467

ISBN-13: 0470616377

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First published over 40 years ago, this was the first text on the identification of organic compounds using spectroscopy. This text is now considered to be a classic. This text presents a unified approach to the structure determination of organic compounds based largely on mass spectrometry, infrared (IR) spectroscopy, and multinuclear and multidimensional nuclear magnetic resonance (NMR) spectroscopy. The key strength of this text is the extensive set of practice and real-data problems (in Chapters 7 and 8). Even professional chemists use these spectra as reference data. Spectrometric Identification of Organic Compounds is written by and for organic chemists, and emphasizes the synergistic effect resulting from the interplay of the spectra. This book is characterized by its problem-solving approach with extensive reference charts and tables. The 8th edition of this text maintains its student-friendly writing style - wording throughout has been updated for consistency and to be more reflective of modern usage and methods. Chapter 3 on proton NMR spectroscopy has been overhauled and updated. Also, new information on polymers and phosphorus functional groups has been added to Chapter 2 on IR spectroscopy.

Structure Determination of Organic Compounds

Author: Ernö Pretsch

Publisher: Springer Science & Business Media

Published: 2000

Total Pages: 444

ISBN-13: 9783540678151

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Table -- Combination tables -- 13C NMR spectroscopy -- 1H NMR specroscopy -- IR spectroscopy -- Mass spectrometry -- UV/Vis spectroscopy.

Tables of Spectral Data for Structure Determination of Organic Compounds

Author: Ernö Pretsch

Publisher: Springer Science & Business Media

Published: 2013-06-29

Total Pages: 325

ISBN-13: 3662224550

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Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.

Spectrometric Identification of Organic Compounds

Author: Robert M. Silverstein

Publisher:

Published: 1991-03-06

Total Pages: 440

ISBN-13:

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Teaches the use of the complementary information afforded by four types of spectrometry for identification of organic compounds: mass, infrared, nuclear magnetic resonance, and ultra violet spectrometry. Throughout, the emphasis is on the relationship between chemical structure and spectral response of the molecule. Each chapter includes problems to facilitate student comprehension and demonstrate practical aspects of the material. Also provided are extensive reference material in charts and tables at the end of each chapter, solved problems, and 50 sets of Spectra of Compounds to be identified. In addition to extensive updating, the Fifth Edition includes a new chapter on New Dimensions in NMR Spectrometry.

Guide to Spectroscopic Identification of Organic Compounds

Author: Karen Feinstein

Publisher: CRC Press

Published: 2018-02-06

Total Pages: 140

ISBN-13: 1351443593

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Guide to Spectroscopic Identification of Organic Compounds is a practical "how-to" book with a general problem-solving algorithm for determining the structure of a molecule from complementary spectra or spectral data obtained from MS, IR, NMR, or UV spectrophotometers. Representative compounds are analyzed and examples are solved. Solutions are eclectic, ranging from simple and straightforward to complex. A picture of the relationship of structure to physical properties, as well as to spectral features, is provided. Compounds and their derivatives, structural isomers, straight-chain molecules, and aromatics illustrate predominant features exhibited by different functional groups. Practice problems are also included. Guide to Spectroscopic Identification of Organic Compounds is a helpful and convenient tool for the analyst in interpreting organic spectra. It may serve as a companion to any organic textbook or as a spectroscopy reference; its size allows practitioners to carry it along when other tools might be cumbersome or expensive.

Structural Identification of Organic Compounds with Spectroscopic Techniques

Author: Yong-Cheng Ning

Publisher: Wiley-VCH

Published: 2005-05-06

Total Pages: 480

ISBN-13:

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Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.

SPECTROMETRIC IDENTIFICATION OF ORGANIC COMPOUNDS, 6TH ED

Author: Robert Silverstein & Francis Webster

Publisher: John Wiley & Sons

Published: 2006-09

Total Pages: 500

ISBN-13: 9788126509720

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Market_Desc: Organic and Analytical in the Forensics, Chemical and Pharmaceutical Industries Special Features: · A how-to, hands-on teaching manual· Considerably expanded NMR coverage--NMR spectra can now be interpreted in exquisite detail· New chapters on correlation NMR spectrometry (2-D NMR) and spectrometry of other important nuclei· Uses a problem-solving approach with extensive reference charts and tables· An extensive set of real-data problems offers a challenge to the practicing chemist About The Book: The book provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry.

Spectroscopic Methods in Organic Chemistry

Author: Dudley H. Williams

Publisher: McGraw-Hill Companies

Published: 1980

Total Pages: 268

ISBN-13:

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Interpretation of Organic Spectra

Author: Yong-Cheng Ning

Publisher: John Wiley & Sons

Published: 2011-04-18

Total Pages: 426

ISBN-13: 0470828315

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Although there are a number of books in this field, most of them lack an introduction of comprehensive analysis of MS and IR spectra, and others do not provide up-to-date information like tandem MS. This book fills the gap. The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5). In each chapter the author presents very practical application skills by providing various challenging examples. The last chapter (Chapter 6) provides the strategy, skills and methods on how to identify an unknown compound through a combination of spectra. Based on nearly 40 years researching and teaching experience, the author also proposes some original and creative ideas, which are very practical for spectral interpretation.