Radiochemical Methods in Analysis

Radiochemical Methods in Analysis PDF

Author: D. Coomber

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 502

ISBN-13: 1461344018

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The aim of this book is to give an account of the principal radiochemical methods used in chemical analysis. It is assumed that the reader already has some background knowledge of radioactivity, available from several general textbooks. For this reason some subjects, e. g. the fundamentals of radio activity, the properties of radiation, statistics of counting procedures, the precautions needed in working with radioactive materials, which could have occupied half the text, are not considered in detail. The different aspects of radiochemical analysis have been covered by specialized books and reviews, e. g. on activation analysis, gamma spectrometry, radiometric titrations. A good deal of information is in the form of reports of meetings and symposia and liquid scintillation counting, for instance, has been mainly covered in this way. There are also a large number of journals. It is therefore hoped that this book will help fill the gap between the introductory texts and the specialized sources, many of which are referred to in the chapter references. The ftrst three chapters in the present volume deal with the methods of measurement of radioactive nuclides. Chapter I gives a general account of detection and measurement techniques. The next two chapters are devoted to two specialized techniques: gamma-ray spectrometry and liquid scintilla tion counting.

Radiochemical Methods

Radiochemical Methods PDF

Author: William J. Geary

Publisher: John Wiley & Sons

Published: 1986

Total Pages: 262

ISBN-13: 9780471911173

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This book presents the analytical uses of radioactive isotopes within the context of radiochemistry as a whole. It is designed for scientists with relatively little background knowledge of the subject. Thus the initial emphasis is on developing the basic concepts of radioactive decay, particularly as they affect the potential usage of radioisotopes.

Radiochemistry and Nuclear Methods of Analysis

Radiochemistry and Nuclear Methods of Analysis PDF

Author: William D. Ehmann

Publisher: Wiley-Interscience

Published: 1993-06-24

Total Pages: 0

ISBN-13: 9780471306283

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From nuclear dating methods to nucleosynthesis in stars. it's all here. The first practical, comprehensive guide to the science of radiochemistry. Radiochemistry and Nuclear Methods of Analysis is the first thorough and up-to-date look for the nonspecialist at the fundamentals of radiochemistry as well as the full range of advances currently made possible by the applications of radioactivity. Without an emphasis on high-level mathematics or abstruse theoretical physics, the book provides a clear, fundamentals-first look at radioactivity, the principles of radioactive decay, and nuclear reactions, as well as: * Modern radiochemical instrumentation * Nuclear dating methods * Methods for the production of radionuclides * The use of tracers and nuclear methods of analysis * The origin of the chemical elements * The biological effects of radiation The book's user-friendly instructional format, designed for both beginning and advanced students, includes numerous end-of-chapter problems ranging from the simple to complex which familiarize the reader with equations and concepts in the text. References to recent monographs, available in most college and university libraries, provide direction to more specialized literature. Invaluable to both students and professionals in search of a practical grasp of the subject, Radiochemistry and Nuclear Methods of Analysis is a clear introduction to radioactivity and radionuclear chemistry's principles, methods, and applications.

Radiochemistry and Nuclear Methods of Analysis

Radiochemistry and Nuclear Methods of Analysis PDF

Author: William D. Ehmann

Publisher: Wiley-Interscience

Published: 1991-09-10

Total Pages: 576

ISBN-13:

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From nuclear dating methods to nucleosynthesis in stars. it's all here. The first practical, comprehensive guide to the science of radiochemistry. Radiochemistry and Nuclear Methods of Analysis is the first thorough and up-to-date look for the nonspecialist at the fundamentals of radiochemistry as well as the full range of advances currently made possible by the applications of radioactivity. Without an emphasis on high-level mathematics or abstruse theoretical physics, the book provides a clear, fundamentals-first look at radioactivity, the principles of radioactive decay, and nuclear reactions, as well as: * Modern radiochemical instrumentation * Nuclear dating methods * Methods for the production of radionuclides * The use of tracers and nuclear methods of analysis * The origin of the chemical elements * The biological effects of radiation The book's user-friendly instructional format, designed for both beginning and advanced students, includes numerous end-of-chapter problems ranging from the simple to complex which familiarize the reader with equations and concepts in the text. References to recent monographs, available in most college and university libraries, provide direction to more specialized literature. Invaluable to both students and professionals in search of a practical grasp of the subject, Radiochemistry and Nuclear Methods of Analysis is a clear introduction to radioactivity and radionuclear chemistry's principles, methods, and applications.

Radiochemical Analysis

Radiochemical Analysis PDF

Author: James R. DeVoe

Publisher:

Published: 1966

Total Pages: 244

ISBN-13:

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NBS activities in the following areas are reported: Activation analysis (facilities, analyses with nuclear reactor, photon activation analysis using the NBS linac, experimental design in activation analysis, radiochemical separations); Instrumentation (interface units, time of year (TOY) system, time mode control unit, data logging system, fast rise preamplifier, solid-state detector systems, observations on calibration of a pulse height analyzer using a sodium iodide detector, pneumatic transport system rabbit sensor); Radiation techniques (Mossbauer spectroscopy); Radioisotope techniques (facilities, the application of radioactive isotopes to the quantitative analysis of trace amounts of inorganic substances on paper and thin layer chromatograms, differential controlled-potential coulometry utilizing radioisotopic tracers, radioisotopic dilution for trace chemical analysis). Also included are: Notes on the use of the G. E. time-sharing computer for multicomponent decay curve analysis; FORTRAN program for analysis of Mossbauer spectra.

Handbook of Radioactivity Analysis

Handbook of Radioactivity Analysis PDF

Author: Michael F. L'Annunziata

Publisher: Elsevier

Published: 2012-12-02

Total Pages: 810

ISBN-13: 0323137881

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Handbook of Radioactivity Analysis is written by experts in the measurement of radioactivity. The book describes the broad scope of analytical methods available and instructs the reader on how to select the proper technique. It is intended as a practical manual for research which requires the accurate measurement of radioactivity at all levels, from the low levels encountered in the environment to the high levels measured in radioisotope research. This book contains sample preparation procedures, recommendations on steps to follow, necessary calculations, computer controlled analysis, and high sample throughput techniques. Each chapter includes practical techniques for application to nuclear safety, nuclear safeguards, environmental analysis, weapons disarmament, and assays required for research in biomedicine and agriculture. The fundamentals of radioactivity properties, radionuclide decay, and methods of detection are included to provide the basis for a thorough understanding of the analytical procedures described in the book. Therefore, the Handbook can also be used as a teaching text. Includes sample preparation techniques for matrices such as soil, air, plant, water, animal tissue, and surface swipes Provides procedures and guidelines for the analysis of commonly encountered na

Radiochemical Analysis

Radiochemical Analysis PDF

Author: James R. DeVoe

Publisher:

Published: 1966

Total Pages: 174

ISBN-13:

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A Mossbauer spectrometer which uses optical interferometry in the Doppler drive, and the mechanical design for the electromechanical drive described in last years report are presented. A description of chemical shift of iron compounds is given. The use of a correction factor for certain source detector geometries are described for Mossbauer spectroscopy. A new source of Sn(119m) in palladium which produces a very narrow line width is also described. For the first time a trace element has been certified in a Standard Reference Material with the assistance of the activation analysis technique. Flux measurements for the NRL reactor are given. A number of special analyses for various NBS projects by activation analysis are described (e.g. argon in silicon, chlorine in polystyrene, hafnium in zirconium). A beta-gamma sum coincidence gamma ray spectrometer is described. A constant potential electrochemical method of analysis using radioisotopic tracers is presented which has potential high sensitivity. A method of using radioisotopic tracers in heterogeneous equilibrium between an aqueous medium of cobalt to be analyzed and manganese dioxide impregnated filter paper is described. Some results on the precision of the substoichiometric radioisotope dilution analysis of silver and iron are presented.

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