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Neutron Diffraction

$Neutron Diffraction PDF$

Author: H. Dachs

Publisher: Springer

Published: 2011-12-15

Total Pages: 0

ISBN-13: 9783642812385

Since the great discovery made by Laue, x-ray diffraction has become the most im portant method for the investigation of atomic structure in condensed matter. Cer tain investigations, however, are difficult or totally impossible to conduct using x-rays, for example, the localization of atomic nuclei or atoms having only a few core electrons, and the observation of magnetic moments. The investigation of these important areas is made possible by neutron diffraction. Thus this method has devel oped into an important supplement to x-ray investigations. An ever-increasing de mand is put on the method by research areas, old and new. Neutron diffraction has completely reformed the subject of solid-state magnetism; especially the area of chemical binding has received a new impetus by the union of x-ray and neutron dif fraction. An exchange of different isotopes of the same element gives rise, as a rule, to a change in the strength of the neutron diffraction. Due to this effect itls possible, by means of deuteration, to make visible a single chain in a solid high polymer. Thus neutron small-angle scattering is important in protein research and for the biology of macromolecules. Of equal importance is the application of neu:ron diffraction in metallurgy. There already exist several excellent books which discuss the results obtained by neans of neutron diffraction.

X-Ray and Neutron Diffraction in Nonideal Crystals

$X-Ray and Neutron Diffraction in Nonideal Crystals PDF$

Author: Mikhail A. Krivoglaz

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 483

ISBN-13: 3642742912

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Mikhail Alexandrovich Krivoglaz died unexpectedly when he was preparing the English edition of his two-volume monograph on diffraction and diffuse scatter ing of X-rays and neutrons in imperfect crystals. His death was a heavy blow to all who knew him, who had worked with him and to the world science community as a whole. The application of the diffraction techniques for the study of imperfections of crystal structures was the major field of Krivoglaz' work throughout his career in science. He started working in the field in the mid-fifties and since then made fundamental contributions to the theory of real crystals. His results have largely determined the current level of knowledge in this field for more than thirty years. Until the very last days of his life, Krivoglaz continued active studies in the physics of diffraction effects in real crystals. His interest in the theory aided in the explanation of the rapidly advancing experimental studies. The milestones marking important stages of his work were the first mono graph on the theory of X-ray and neutron scattering in real crystals which was published in Russian in 1967 (a revised English edition in 1969), and the two volume monograph published in Russian in 1983-84 (this edition is the revised translation of the latter).

Neutron Diffraction of Magnetic Materials

$Neutron Diffraction of Magnetic Materials PDF$

Author: Izyumov

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 349

ISBN-13: 1461536588

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Detennination of the magnetic structure of magnetic materials is a fundamental problem that can be solved by magnetic neutron diffraction techniques. By magnetic structures we refer to the mutual alignment of the magnetic moments of the atoms in a crystal and their overall alignment relative to the crystallographic axes. Some indirect, tentative data on the magnetic structure of magnetic materials can be obtained from research on their magnetic, mechanical, thermal, and other properties. But only neutron diffraction is a unique direct method of detennining the magnetic structure of a crystal. The magnetic structure of more than one thousand crystals with magnetic order has been studied during 30 years of neutron diffraction research made on reactors in a large number of laboratories in the world. The results of this research work are extensively described in the handbook Magnetic Structures Determined by Neutron Diffraction [176]; in the present book, we will often refer to this handbook. The first extensive theoretical generalization of the principles of magnetic neutron diffraction and the results of research on magnetic structures appeared in the book by Yu. A. Izyumov and R. P. Ozerov Magnetic Neutron Diffraction [24, 134].

Magnetic Neutron Diffraction

$Magnetic Neutron Diffraction PDF$

Author: Yurii A. Izyumov

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 607

ISBN-13: 1468407120

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The inter action between the magnetic field generated by the neutron and the magnetic moment of atoms containing unpaired electrons was experimentally demonstrated for the first time about twenty years ago. The basic theory describing such an in teraction had already been developed and the first nuclear reactors with large available thermal neutron fluxes had recently been con structed. The power of the magnetic neutron interaction for in vestigating the structure of magnetic materials was immediately recognized and put to use where possible. Neutron diffraction, however, was practicable only in countries with nuclear reactors. The earliest neutron determinations of magnetic ordering were hence primarily carried out at Oak Ridge and Brookhaven in the US, at Chalk River in Canada and at Harwell in England. Diffraction patterns from polycrystalline ferromagnets and antiferromagnets are interpretable if produced by simple spin arrays. More complex magnetic scattering patterns could often be unravelled, in terms of a three-dimensional array of atomic moments, if the specimen studied is a single crystal. The devel opment of sophisticated cryogenic equipment, with independently alignable magnetic fields, opened the way to greater complexity in the magnetic structures that could be successfully determined, as did also the introduction of polarized neutron beams. By the end of the 'sixties, many countries were contributing significantly to neutron diffraction studies of a wide variety of magnetic materials.

Measurement of Residual and Applied Stress Using Neutron Diffraction

$Measurement of Residual and Applied Stress Using Neutron Diffraction PDF$

Author: M.T. Hutchings

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 568

ISBN-13: 9401127972

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The accurate, absolute, and non-destructive measurement of residual stress fields within metallic, ceramic, and composite engineering components has been one of the major problems facing engineers for many years, and so the extension of X-ray methods to the use of neutrons represents a major advance. The technique utilizes the unique penetrating power of the neutron into most engineering materials, combined with the sensitivity of diffraction, to measure the separation of lattice planes within grains of polycrystalline engineering materials, thus providing an internal strain gauge. The strain is then converted to stress using calibrated elastic constants. It was just over ten years ago that the initial neutron diffraction measurements of residual stress were carried out, and during the ensuing decade measurements have commenced at most steady state reactors and pulsed sources around the world. So swift has been the development of the field that, in addition to fundamental scientific studies, commercial measurements have been made on industrial components for several years now. The use of neutrons is ideally suited to the determination of triaxial macrostress tensors, macrostress gradients, and microstresses in composites and multiphase alloys as well as deformed, plastically anisotropic metals and alloys. To date, it has been used to investigate welded and heat-treated industrial components, to characterize composites, to study the response of material under applied loads, to calibrate more portable methods such as ultrasonics, and to verify computer modelling calculations of residual and applied stress.

Introduction to the Characterization of Residual Stress by Neutron Diffraction

$Introduction to the Characterization of Residual Stress by Neutron Diffraction PDF$

Author: M.T. Hutchings

Publisher: CRC Press

Published: 2005-02-28

Total Pages: 383

ISBN-13: 0203402812

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Over the past 25 years the field of neutron diffraction for residual stress characterization has grown tremendously, and has matured from the stage of trial demonstrations to provide a practical tool with widespread applications in materials science and engineering. While the literature on the subject has grown commensurately, it has also remained

Applications of Neutron Powder Diffraction

$Applications of Neutron Powder Diffraction PDF$

Author: Erich H. Kisi

Publisher: Oxford University Press

Published: 2012-09-27

Total Pages: 509

ISBN-13: 0199657424

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This is the first book covering the theory, practicalities, and the extensive applications of neutron powder diffraction in materials science, physics, chemistry, mineralogy, and engineering. The broad coverage should be accessible to graduate students and senior undergraduates in science and engineering, as well as lecturers and researchers.

X-Ray and Neutron Dynamical Diffraction

$X-Ray and Neutron Dynamical Diffraction PDF$

Author: André Authier

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 419

ISBN-13: 1461558794

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This volume collects the proceedings of the 23rd International Course of Crystallography, entitled "X-ray and Neutron Dynamical Diffraction, Theory and Applications," which took place in the fascinating setting of Erice in Sicily, Italy. It was run as a NATO Advanced Studies Institute with A. Authier (France) and S. Lagomarsino (Italy) as codirectors, and L. Riva di Sanseverino and P. Spadon (Italy) as local organizers, R. Colella (USA) and B. K. Tanner (UK) being the two other members of the organizing committee. It was attended by about one hundred participants from twenty four different countries. Two basic theories may be used to describe the diffraction of radiation by crystalline matter. The first one, the so-called geometrical, or kinematical theory, is approximate and is applicable to small, highly imperfect crystals. It is used for the determination of crystal structures and describes the diffraction of powders and polycrystalline materials. The other one, the so-called dynamical theory, is applicable to perfect or nearly perfect crystals. For that reason, dynamical diffraction of X-rays and neutrons constitutes the theoretical basis of a great variety of applications such as: • the techniques used for the characterization of nearly perfect high technology materials, semiconductors, piezoelectric, electrooptic, ferroelectric, magnetic crystals, • the X-ray optical devices used in all modem applications of Synchrotron Radiation (EXAFS, High Resolution X-ray Diffractometry, magnetic and nuclear resonant scattering, topography, etc. ), and • X-ray and neutron interferometry.

Single Crystal Neutron Diffraction From Molecular Materials

$Single Crystal Neutron Diffraction From Molecular Materials PDF$

Author: Chick C Wilson

Publisher: World Scientific Publishing Company

Published: 2000-02-18

Total Pages: 384

ISBN-13: 9813105402

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This important book presents a comprehensive account of the techniques and applications of single crystal neutron diffraction in the area of chemical crystallography and molecular structure. Beginning with a brief description of the general principles and the reasons for choosing the technique — the “why” — the book covers the methods for both the production of neutrons and the measurement of their scattering by molecular crystals — the “how” — followed by a detailed survey of past, present and future applications — the “what”. The coverage of both steady state and pulsed neutron sources and instrumentation is extensive, while the survey of applications is the most comprehensive yet undertaken. The book endeavours to show why the technique is an essential method for studying areas as diverse as hydrogen bonding and weak interactions, organometallics, supramolecular chemistry and crystal engineering, metal hydrides, charge density and pharmaceuticals. It is an ideal reference source for the research worker interested in using neutron diffraction to study the structure of molecules.

Neutron Scattering in Biology

Author: Jörg Fitter

Publisher: Springer Science & Business Media

Published: 2006-05-01

Total Pages: 571

ISBN-13: 3540291113

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The advent of new neutron facilities and the improvement of existing sources and instruments world wide supply the biological community with many new opportunities in the areas of structural biology and biological physics. The present volume offers a clear description of the various neutron-scattering techniques currently being used to answer biologically relevant questions. Their utility is illustrated through examples by some of the leading researchers in the field of neutron scattering. This volume will be a reference for researchers and a step-by-step guide for young scientists entering the field and the advanced graduate student.