MALDI-TOF Mass Spectrometry of Synthetic Polymers

MALDI-TOF Mass Spectrometry of Synthetic Polymers PDF

Author: Harald Pasch

Publisher: Springer Science & Business Media

Published: 2013-03-09

Total Pages: 312

ISBN-13: 3662050463

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MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.

MALDI Mass Spectrometry for Synthetic Polymer Analysis

MALDI Mass Spectrometry for Synthetic Polymer Analysis PDF

Author: Liang Li

Publisher: John Wiley & Sons

Published: 2009-10-22

Total Pages: 325

ISBN-13: 0470567228

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Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization. It discusses different approaches, including MALDI, ESI, TOF MS, and FT-MS. It provides a guide to developing appropriate sample preparation protocols for different polymers. Complete with examples of applications and experiments, this is an excellent reference for scientists, researchers, graduate students, and others.

MALDI Mass Spectrometry for Synthetic Polymer Analysis

MALDI Mass Spectrometry for Synthetic Polymer Analysis PDF

Author: Liang Li

Publisher: Wiley

Published: 2009-12-09

Total Pages: 307

ISBN-13: 9780471775799

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Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization. It discusses different approaches, including MALDI, ESI, TOF MS, and FT-MS. It provides a guide to developing appropriate sample preparation protocols for different polymers. Complete with examples of applications and experiments, this is an excellent reference for scientists, researchers, graduate students, and others.

Mass Spectrometry of Polymers

Mass Spectrometry of Polymers PDF

Author: Giorgio Montaudo

Publisher: CRC Press

Published: 2001-10-29

Total Pages: 601

ISBN-13: 1420037757

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Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results

Mass Spectrometry of Polymers

Mass Spectrometry of Polymers PDF

Author: Giorgio Montaudo

Publisher: CRC Press

Published: 2001-10-29

Total Pages: 771

ISBN-13: 1000611515

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Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results

Mass Spectrometry in Polymer Chemistry

Mass Spectrometry in Polymer Chemistry PDF

Author: Christopher Barner-Kowollik

Publisher: John Wiley & Sons

Published: 2012-01-27

Total Pages: 501

ISBN-13: 3527641831

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Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.

Fundamentals of MALDI-ToF-MS Analysis

Fundamentals of MALDI-ToF-MS Analysis PDF

Author: Samira Hosseini

Publisher: Springer

Published: 2016-08-18

Total Pages: 68

ISBN-13: 9811023565

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This book presents the fundamentals and applications of Matrix Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry (MALDI-ToF-MS) technique. It highlights the basic principles, the history of invention as well as the mechanism of ionization and mass determination using this technique. It describes the fundamental principles and methods for MALDI spectra interpretation and determination of exact chemical structures from experimental data. This book guides the reader through the interpretation of MALDI data where complex macromolecular spectra are simplified in order to present the major principles behind data interpretation. In addition, each chapter describes how MALDI-ToF-MS analysis provides necessary understanding of the copolymer systems that have been designed for specialized biomedical applications.

Liquid Chromatography of Synthetic Polymers

Liquid Chromatography of Synthetic Polymers PDF

Author: Muhammad Imran Malik

Publisher: Springer Nature

Published: 2023-11-03

Total Pages: 310

ISBN-13: 3031348354

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This book elucidates the peculiar phenomenon of entropy/enthalpy compensation that takes place in high performance liquid chromatography (HPLC) of polymers. Numerous publications, including some books, are devoted to molecular characterization of synthetic polymers, materials presently produced in large and steadily growing quantities, applying methods of HPLC. A knowledge of the molecular characteristics of polymers is indispensable, not only for their proper applications but also for their recycling and remediation. Polymer scientists generally focus on synthesis and potential applications of polymers while not giving due attention to an important central link, their comprehensive characterization in context of development of structure-property correlations. To fill this gap is one of the aims of the present book. The process of entropy/enthalpy compensation plays a decisive role in the advanced method of polymer characterization such as liquid chromatography at critical conditions, eluent gradient interaction chromatography, and temperature gradient interaction chromatography. All chemists working on any aspect of polymer science will find this book a valuable resource for the development of structure-property correlations.

Mass Spectrometry of Polymers – New Techniques

Mass Spectrometry of Polymers – New Techniques PDF

Author: Minna Hakkarainen

Publisher: Springer Science & Business Media

Published: 2012-03-14

Total Pages: 219

ISBN-13: 3642280412

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Emerging Mass Spectrometric Tools for Analysis of Polymers and Polymer Additives, by Nina Aminlashgari and Minna Hakkarainen. Analysis of Polymer Additives and Impurities by Liquid Chromatography/Mass Spectrometry and Capillary Electrophoresis/Mass Spectrometry, by Wolfgang Buchberger and Martin Stiftinger. Direct Insertion Probe Mass Spectrometry of Polymers, by Jale Hacaloglu Mass Spectrometric Characterization of Oligo- and Polysaccharides and Their Derivatives, by Petra Mischnick. Electrospray Ionization-Mass Spectrometry for Molecular Level Understanding of Polymer Degradation, by Minna Hakkarainen.

Orthogonal Fractional Factorial Designs

Orthogonal Fractional Factorial Designs PDF

Author: Aloke Dey

Publisher:

Published: 1985-09-30

Total Pages: 152

ISBN-13:

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A systematic and up-to-date account of fractional factorial designs giving uncorrelated estimates of relevant parameters. After basic concepts of design and analysis of factorial experiments are introduced, consideration is given to a detailed account of all available methods of obtaining orthogonal fractional factorial designs. Both symmetrical and asymmetrical pictorials are covered. Features an extensive table giving an index of fractional factorial designs. All recent work, including that unpublished, is included, and references provided.