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Author: A. Mersmann
Publisher: CRC Press
Published: 2001-05-08
Total Pages: 847
ISBN-13: 0824745116
DOWNLOAD EBOOK →This handbook seeks to facilitate the selection, design and operation of large-scale industrial crystallizers that process crystals with the proper size distribution, shape and purity sought. This second edition offers results on direct-contact cooling crystallization.
Author: G L Strathdee
Publisher: Elsevier
Published: 2016-12-05
Total Pages: 332
ISBN-13: 1483191109
DOWNLOAD EBOOK →Crystallization and Precipitation is a collection of papers that discusses the advancement in crystallization and precipitation technology. The titles assess the relative state of evolution of the science, engineering and practice in crystallization and precipitation. The coverage of the text includes chemical reactor approach to crystallizer analysis; uranium refining by uranyl nitrate hexahydrate crystallization; and valorization of liquid effluents by crystallization of sodium sulfate. The selection also covers precipitation of ferric arsenate from acid solutions; precipitation of silver on natural and synthetic sulphides theory and prospects of industrial use; and precipitation and its alternatives in the hydrometallurgy of gold. The book will be of great use to researchers and professionals who utilizes the mineral processes of crystallization and precipitation.
Author: Allan Myerson
Publisher: Butterworth-Heinemann
Published: 2002-01-08
Total Pages: 329
ISBN-13: 0080533515
DOWNLOAD EBOOK →Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes.The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design. Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the fieldCovers all aspects of industrial crystallization in a single, complete volume
Author: Alison Lewis
Publisher: Cambridge University Press
Published: 2015-07-02
Total Pages: 354
ISBN-13: 1316299082
DOWNLOAD EBOOK →Bridging the gap between theory and practice, this text provides the reader with a comprehensive overview of industrial crystallization. Newcomers will learn all of the most important topics in industrial crystallization, from key concepts and basic theory to industrial practices. Topics covered include the characterization of a crystalline product and the basic process design for crystallization, as well as batch crystallization, measurement techniques, and details on precipitation, melt crystallization and polymorphism. Each chapter begins with an introduction explaining the importance of the topic, and is supported by homework problems and worked examples. Real world case studies are also provided, as well as new industry-relevant information, making this is an ideal resource for industry practitioners, students, and researchers in the fields of industrial crystallization, separation processes, particle synthesis, and particle technology.
Author: Alan G. Jones
Publisher: Butterworth-Heinemann
Published: 2002-04-24
Total Pages: 362
ISBN-13: 0750655208
DOWNLOAD EBOOK →Particulate Crystal Characteristics; Fluid-particle Transport Processes; Crystallization Principles and Techniques; Crystal Formation Processes; Crystallizer Design and Operation; Solid-Liquid Separation Processes; Design of Crystallization Process Systems.
Author: Otakar Söhnel
Publisher: Butterworth-Heinemann
Published: 1992
Total Pages: 422
ISBN-13:
DOWNLOAD EBOOK →In this book the authors have drawn together theoretical and experimental material concerning precipitation to provide a uniform and coherent picture of the overall process. The focus is mainly on aqueous solutions and covers features common to all precipitation processes rather than individual cases. Considerable emphasis has been placed on developing a rigorous theoretical background to the kinetics of precipitation as well as attempting to demonstrate how this might be applied to industrial operations. Extensive tables in the appendices define the solubility products of inorganic substances, the surface energies of precipitated solids and solution concentration units.
Author: E. Goldberg
Publisher: Springer Science & Business Media
Published: 2012-12-06
Total Pages: 745
ISBN-13: 9400915632
DOWNLOAD EBOOK →The last two decades have seen a phenomenal growth of the field of genetic or biochemical engineering and have witnessed the development and ultimately marketing of a variety of products-typically through the manipulation and growth of different types of microorganisms, followed by the recovery and purification of the associated products. The engineers and biotechnologists who are involved in the full-scale process design of such facilities must be familiar with the variety of unit operations and equipment and the applicable regulatory requirements. This book describes current commercial practice and will be useful to those engineers working in this field in the design, construction and operation of pharmaceutical and biotechnology plants. It will be of help to the chemical or pharmaceutical engineer who is developing a plant design and who faces issues such as: Should the process be batch or continuous or a combination of batch and continuous? How should the optimum process design be developed? Should one employ a new revolutionary separation which could be potentially difficult to validate or use accepted technology which involves less risk? Should the process be run with ingredients formulated from water for injection, deionized water, or even filtered tap water? Should any of the separations be run in cold rooms or in glycol jacketed lines to minimize microbial growth where sterilization is not possible? Should the process equipment and lines be designed to be sterilized in-place, cleaned-in-place, or should every piece be broken down, cleaned and autoclaved after every turn?
Author: Marcello Andreeta
Publisher: BoD – Books on Demand
Published: 2012-09-19
Total Pages: 582
ISBN-13: 9535107577
DOWNLOAD EBOOK →Crystallization is one of the most ancient and interdisciplinary topics of research known to mankind. Crystals can be organic or inorganic and may be produced from melts, liquid solutions, vapors or even in solid state. Notwithstanding its inherently high complexity, the crystallization process is part of our everyday lives, from ice making in our homes to the most state-of-the-art chemical and electronic industry. In this book, our purpose was to present new insights to the reader, as well as crucial and very useful information for researchers working in this field, while simultaneously creating a comprehensive text about crystallization processes which may serve as a starting point for people with different backgrounds.
Author: Wolfgang Beckmann
Publisher: John Wiley & Sons
Published: 2013-01-14
Total Pages: 370
ISBN-13: 3527650342
DOWNLOAD EBOOK →Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.
