Basics of Flow Microreactor Synthesis

Basics of Flow Microreactor Synthesis PDF

Author: Jun-ichi Yoshida

Publisher: Springer

Published: 2015-05-08

Total Pages: 111

ISBN-13: 4431555137

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This book provides in a concise form the principles and applications of flow microreactors in organic and polymer synthesis. Recently, it became possible to conduct chemical reactions in a flow reactor in laboratory synthesis. The flow microreactor enables reactions that cannot be done in batch, opening a new possibility of chemical synthesis. Extremely fast mass and heat transfer and high-resolution residence time control are responsible for the remarkable features of that process. The book is not an exhaustive compilation of all known examples of flow microreactor synthesis. Rather, it is a sampling of sufficient variety to illustrate the concept, the scope, and the current state of flow microreactor synthesis. Researchers both in academia and in industry will be interested in this book because the topics encompassed by the book are vigorously studied in many university and company laboratories today.

Flow Chemistry – Fundamentals

Flow Chemistry – Fundamentals PDF

Author: Ferenc Darvas

Publisher: Walter de Gruyter GmbH & Co KG

Published: 2021-10-25

Total Pages: 568

ISBN-13: 3110693771

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The fully up-dated edition of the two-volume work covers both the theoretical foundation as well as the practical aspects. Presenting the complete insight into driving a chemical reaction provides a deep understanding for new potential technologies. Updated overview on devices and new key concepts of experimental procedures. Vol. 2: Applications.

Flash Chemistry

Flash Chemistry PDF

Author: Jun-ichi Yoshida

Publisher: John Wiley & Sons

Published: 2008-10-13

Total Pages: 244

ISBN-13: 0470723416

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Have you ever wished you could speed up your organic syntheses without losing control of the reaction? Flash Chemistry is a new concept which offers an integrated scheme for fast, controlled organic synthesis. It brings together the generation of highly reactive species and their reactions in Microsystems to enable highly controlled organic syntheses on a preparative scale in timescales of a few seconds or less. Flash Chemistry: Fast Organic Synthesis in microsystems is the first book to describe this exciting new technique, with chapters covering: an introduction to flash chemistry reaction dynamics: how fast is the act of chemical transformation, what is the rate of reaction, and what determines the selectivity of a reaction? examples of why flash chemistry is needed: the rapid construction of chemical libraries, rapid synthesis of radioactive PET probes, and on-demand rapid synthesis in industry the generation of highly reactive species through thermal, microwave, chemical, photochemical, and electrochemical activation microsystems: What are microsystems and how are they made? Why is size so important? What are the characteristic features of microsystems? conduction and control of extremely fast reactions using microsystems applications of flash chemistry in organic synthesis polymer synthesis based on flash chemistry industrial applications of flash chemistry Flash Chemistry: Fast Organic Synthesis in Microsystems is an essential introduction to anyone working in organic synthesis, process chemistry, chemical engineering and physical organic chemistry concerned with fundamental aspects of chemical reactions an d synthesis and the production of organic compounds.

Flow Chemistry – Fundamentals

Flow Chemistry – Fundamentals PDF

Author: Ferenc Darvas

Publisher: Walter de Gruyter GmbH & Co KG

Published: 2014-08-25

Total Pages: 307

ISBN-13: 3110388758

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"Flow Chemistry fills the gap in graduate education by covering chemistry and reaction principles along with current practice, including examples of relevant commercial reaction, separation, automation, and analytical equipment. The Editors of Flow Chemistry are commended for having taken the initiative to bring together experts from the field to provide a comprehensive treatment of fundamental and practical considerations underlying flow chemistry. It promises to become a useful study text and as well as reference for the graduate students and practitioners of flow chemistry." Professor Klavs Jensen Massachusetts Institute of Technology, USA Broader theoretical insight in driving a chemical reaction automatically opens the window towards new technologies particularly to flow chemistry. This emerging concept promotes the transformation of present day's organic processes into a more rapid continuous set of synthesis operations, more compatible with the envisioned sustainable world. These two volumes Fundamentals and Applications provide both the theoretical foundation as well as the practical aspects.

Micro Reaction Technology in Organic Synthesis

Micro Reaction Technology in Organic Synthesis PDF

Author: Charlotte Wiles

Publisher: CRC Press

Published: 2016-04-19

Total Pages: 453

ISBN-13: 143982472X

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While continuous processes have found widespread application within chemical production, members of the research and development communities have historically favored the centuries old technique of iterative batch reactions. With the exception of combinatorial and microwave chemistry, little had been done to change the way that synthetic chemists c

Ewing's Analytical Instrumentation Handbook, Fourth Edition

Ewing's Analytical Instrumentation Handbook, Fourth Edition PDF

Author: Nelu Grinberg

Publisher: CRC Press

Published: 2019-02-21

Total Pages: 975

ISBN-13: 1482218682

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This handbook is a guide for workers in analytical chemistry who need a starting place for information about a specific instrumental technique. It gives a basic introduction to the techniques and provides leading references on the theory and methodology for an instrumental technique. This edition thoroughly expands and updates the chapters to include concepts, applications, and key references from recent literature. It also contains a new chapter on process analytical technology.

Continuous-Flow Chemistry in the Research Laboratory

Continuous-Flow Chemistry in the Research Laboratory PDF

Author: Toma Glasnov

Publisher: Springer

Published: 2016-06-01

Total Pages: 119

ISBN-13: 331932196X

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This book presents a short introduction to the historical background to the field, the state of the art and a brief survey of the available instrumentation and the processing techniques used. The following major areas of interest in synthetic, organic and medicinal chemistry are elaborated on: transition-metal catalyzed reactions, organocatalytic transformations, heterocyclic synthesis, and photochemical reactions. Finally, selected applications in industry are also discussed. With its ample presentation of examples from recent literature, this is an essential and reliable source of information for both experienced researchers and postgraduate newcomers to the field.

Science of Synthesis: Flow Chemistry in Organic Synthesis

Science of Synthesis: Flow Chemistry in Organic Synthesis PDF

Author: T.F. Jamison

Publisher: Thieme

Published: 2018-12-12

Total Pages: 932

ISBN-13: 3132423343

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The aim of this work is to convey the practice, power, and potential of flow chemistry to a larger audience. An emerging and strengthening trend is that flow chemistry is much more than the adaption of batch processes to flow systems. Rather, flow chemistry offers a new paradigm in the way we think about chemical synthesis. This volume demonstrates the enabling power of continuous flow to access new reaction types and different chemistry space and, to this end, it has been compiled by a team of pioneers and leaders, who present both the practical and conceptual aspects of this rapidly growing field. Included are the principles of reactor design, automation, and separations/purifications in flow systems, applications in photochemistry, electrochemistry, gaseous systems, immobilized reagents and catalysts, and multistep processes. The synthesis of peptides, carbohydrates, and pharmaceuticals is covered and several chapters give insight into the use of flow in an industrial context.

Middle Molecular Strategy

Middle Molecular Strategy PDF

Author: Koichi Fukase

Publisher: Springer Nature

Published: 2021-07-13

Total Pages: 357

ISBN-13: 9811624585

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This book highlights recently discovered aspects of “middle-size molecules,” focusing on (1) their unique bio-functions on the basis of derivatives and conjugates of natural products, saccharides, peptides, and nucleotides; (2) the synthesis of structurally complex natural products; (3) special synthetic methods for π-conjugated functional molecules; and (4) novel synthetic methods using flow chemistry. Given its scope, the book is of interest to industrial researchers and graduate students in the fields of organic chemistry, medicinal chemistry, and materials science.

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